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Meet Longtime IBM/Brookhaven Lab Scientist Jean Jordan-candy | C1000-010 Cheatsheet and Free PDF

Jordan-sweet retired after a virtually 40-year profession based at Brookhaven Lab

December 1, 2021

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This image indicates Jean Jordan-candy with the microbeam setup at beamline X20A at NSLS in 2001.

prior to her retirement in August, Jean Jordan-candy turned into a senior engineer at IBM analysis and a beamline scientist at the Beamline for substances dimension at countrywide Synchrotron easy supply II (NSLS-II), a U.S. department of power (DOE) user Facility observed at DOE’s Brookhaven countrywide Laboratory. For almost 40 years, her work has focused on the usage of x-ray suggestions to look at materials and techniques for the advancement of microelectronics technologies.

What brought you to Brookhaven Lab initially of your career?

I first got here to Brookhaven Lab about 40 years ago as a grad pupil from the institution of California at l. a. (UCLA) and did some of my thesis experiments right here.

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Jean Jordan-sweet is looking forward to proceed working with the country wide Institute of standards and know-how (NIST) at NSLS-II after her departure from IBM in 2021.

My marketing consultant at UCLA, John McTague, had been a collaborator on a assignment using x-rays at early synchrotrons to look at adsorbed inert gas films, which kind two dimensional phases. at the moment, the brightness of x-rays wasn’t first rate ample to look at a single surface the manner they will now, so they had to make substrates that had been in powder form. the use of a powder intended having lots of small crystals that together had ample floor area to get a signal from the adsorbed movie. My thesis involved making a excessive-floor-area powder substrate that had a special symmetry. So, I made magnesium oxide (MgO) powder, which has rectangular floor symmetry. I used a rotating anode x-ray source at Brookhaven to study the two-dimensional melting of krypton adsorbed on MgO. That source became owned by means of Dave Moncton, who became a collaborator with my guide. I used that instrument 24/7 for a couple of weeks to take my thesis records.

We additionally collaborated with Larry Passell, who was my mentor here at Brookhaven Lab and part of the Condensed remember Physics branch. he is a gorgeous man and that i get pleasure from travelling him to today. I analyzed all my thesis data with his support and graduated in 1983. I then bought a postdoc with IBM on the ultraviolet (UV) section of the country wide Synchrotron gentle source (NSLS), the predecessor of NSLS-II. I all started out by way of discovering polymer/steel interfaces the use of UV spectroscopy. From there, it was a natural progression to practice for a job to run IBM’s x-ray diffraction beamlines at NSLS. In 1986, i was hired through IBM permanently to do exactly that.

What become your work like in these early years at NSLS?

in the late 80s, industry claimed a huge fraction of NSLS beamlines; there have been Exxon, Bell Labs, and Dow/Dupont, for instance. IBM had about seven beamlines at NSLS, and that they all did various things. a couple did x-ray lithography, two were for x-ray diffraction, and there turned into a set of beamlines for optics construction and ultraviolet spectroscopy.

IBM firstly entered right into a associate-oriented operational mode at NSLS, specially to be in a position to control what form of instrumentation they developed and had entry to. They had been participating with scientists on the Massachusetts Institute of expertise (MIT), the place they did a lot of condensed be counted physics research and IBM did a lot of microelectronics-connected analysis. lower back then it changed into particularly cost effective to put a beamline together. They operated the X20 diffraction beamlines until the conclusion of NSLS.

What scientific questions drove your analysis?

in the early days of my profession, IBM became a very vertically-integrated business. They did every little thing, from making the chips to constructing the shows and the complicated drives. They had been simply starting to make PCs at that time. So, there were loads of distinctive substances to analyze with x-rays, such because the orientation of the liquid crystals utilized in flat-panel shows, and the part materials that make up microprocessors and storage devices.

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Jean Jordan-sweet (in the lower back) with three other researchers proven right here taking records at the X20C beamline at NSLS. picture courtesy of Jean Jordan-candy.

a lot of the measurements they took have been geared toward understanding the behavior and traits of skinny films or stacks of thin films. for those who make a chip, it’s bought a whole bunch of diverse layers. each layer is deposited and processed in response to some recipe, whether it’s implanted, annealed and/or etched. So, there are a variety of materials and approaches to look at. They may use x-rays to do all sorts of measurements.

currently, IBM is concentrating on very superior computation like synthetic intelligence (AI), neuromorphic computing, and quantum computing, so they boost very high-conclusion hardware. IBM is looking at completely alternative ways of doing computation, similar to using reminiscence as a computing gadget for AI. These tactics are more analog than digital because you are trying to mimic the synaptic pathways of a mind. those architectures contain a whole diverse set of materials.

Then there is quantum computing. That hardware is fully different and includes a further set of substances operating at ultra-low temperatures. we've practically the whole periodic desk to play with.

How did you turn into drawn to this work?

In excessive college, I had a very good physics trainer, and he received me considering a few career in science. Then in faculty, I double-majored in physics and chemistry. I also did a few countrywide Science basis summer programs: One when i used to be a junior in excessive faculty, and the different when i used to be a junior in school. The one all the way through school become at Argonne national Laboratory. i was taking a tour of Chicago Pile-5, which became the ultimate version of their nuclear reactor for science analysis. i was looking around on the measurement of the instruments and the entire neat stuff; it become like a beehive in there. and that i thought, wow, it would be so cool to work at a place like this.

What have you been working on these days?

just before my retirement, I worked at the Beamline for materials Measurements, also called BMM, which is led with the aid of Bruce Ravel, and they signed a CRADA with the countrywide Institute of specifications and technology (NIST) to place an x-ray diffraction conclusion station in the downstream end of Bruce’s hutch. IBM gets about one-sixth of the beamtime for experiments, where they do commonly diffraction and x-ray reflectivity. They even have used the spectroscopy capabilities to support us discover samples now not with no trouble characterised with x-ray diffraction.

BMM is a phenomenal source for us. Bruce has it so smartly programmed; I by no means must calibrate the energy and it well-nigh aligns itself. It’s been a pleasure working there. The source at NSLS-II is so strong, with a relentless beam depth, that it’s plenty less demanding to do experiments here than at NSLS.

A paper that they posted this yr become about attempting to take note the crystal structure of skinny hafnium oxide films which have been doped to develop into ferroelectric. This cloth is a candidate for an extra kind of memory — ferroelectric reminiscence — it is being developed for neuromorphic computing. no person had yet definitively decided the constitution of the ferroelectric part. Oxides like these have peaks in every single place on an x-ray diffraction plot and it’s actually difficult to pin down what the constitution is. At BMM, together with colleagues from IBM, NIST, and Seton corridor tuition, they used x-ray absorption spectroscopy at NSLS-II and density useful theory modelling to truly pin down the structure of that ferroelectric phase. They nailed it and posted a paper in utilized Physics Letters.

What are some highlights of your career?

I think, for IBM, their most impactful building become the thermal annealing x-ray diffraction equipment, which is a totally really expert chamber established on a diffractometer. Thermal processing of layers is likely one of the most ordinary steps in chip manufacturing. In their gadget, thin movie or patterned samples on wafer items are clamped onto a heater the use of what's known as a 4-factor probe, which measures electrical resistance in a film. X-rays diffract from the film onto a linear detector while the pattern is being promptly heated to a desired temperature. They additionally had a laser that would replicate off the surface and scatter, and the intensity of the scattered light would let you know how rough the surface became on a number of length scales. This finished device allowed us to measure temperature and kinetics of phase formation or crystallization counting on a large number of variables, reminiscent of dopants introduced, deposition system, substrate used, etc.

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Brookhaven Lab is a family unit affair for the Sweets, as proven during this photo of Alan, Jean, Bob, and Marie taken right through a poster session of Brookhaven's summer time intern program in 2011, whereas they are conserving a photograph taken at the 45th Brookhaven Lab anniversary picnic in 1994. Bob works within the structural biology software at NSLS-II.

We used that approach to seem at the formation of the little contact pads that are a part of the wiring on a computer chip; they are referred to as self-aligned silicides and are shaped with the aid of reacting metal with the underlying semiconducting areas that form the transistor gate, source, and drain. it's vital that these contacts have very low resistance since you are bringing a low voltage signal in and out. through the years they studied a whole lot metallic films on distinct semiconductors, creating an enormous database of what buildings had been shaped under a number of circumstances — 35,000 facts runs in total.

throughout the ultimate years of NSLS operations, when IBM was using nickel silicide as a contact pad, they found out that their manufacturing yield for a brand new processor chip changed into terrible. a big mass of nickel silicide (NiSi) every now and then formed appropriate in the carrier channel and shorted out the transistors. It turned into referred to as the “NiSi fang defect” since it changed into formed like a fang. They pinpointed the trigger through searching on the geometry of the machine, relating to their big database, and doing some extra measurements on their instrument. The difficulty changed into solved by means of including a 2nd annealing step that converted some Ni-prosperous silicide created during an etching step lower back to NiSi. IBM had been dealing with a months-lengthy prolong in the sale of a new technology of servers and averting that turned into a huge deal.

We bought an IBM research fantastic Technical fulfillment award for that, which is putting on my wall.

What became it like to navigate the end of NSLS and the beginning of NSLS-II?

The gap between NSLS and NSLS-II become tough. It was a loopy time. They did some runs as ordinary clients at different synchrotrons. but I needed to take apart their old X20 beamlines, work out who to donate stuff to, clear it up, crate it, and ship it out. It took a yr to get all that performed. They shipped out virtually 15 hundreds device! And at that time, right earlier than the NSLS shut down, they also had developed and commissioned an automated annealing/x-ray diffraction end station that became despatched as much as the Canadian light source. That additionally had to be crated and shipped out.

“closing easy” at NSLS changed into complicated. Some managers got here down from IBM, in addition to a few of their collaborators, and it was truly quality that they wanted to witness it. i was in fact taking a dimension there on the very conclusion. It’s known as a pole figure, which is a way to measure microcrystalline film texture. It took two and a half hours to try this, it was a whole sequence of scans. I remember watching the clock tick down. The experiment accomplished about 30 seconds before they did the remaining beam dump.

Did you appreciate your years at the Brookhaven Lab’s easy sources?

typical, very a lot so. The team of workers is wonderful, my collaborators were astonishing. I’ve been so impressed over the years with how smart the americans are who come here and the fantastic tasks they work on.

I’ve been very lucky, as a result of what's the likelihood of business supporting a person working at a country wide lab for 37 years? It’s been a superb run! I recognize that IBM has recognized the value of this analysis and supplied for me to stay right here for my total profession.

what is subsequent for you?

I’m hoping that i will be able to nevertheless retain my foot within the door. In February, they introduced in Vesna Stanic to take my location working the IBM end station at NSLS-II, and she or he is terribly first rate at that. She has a whole lot of synchrotron event, but she’s nevertheless now not absolutely universal with the entire instrumentation that I put together. We’ve only carried out three runs collectively on account that she arrived. So, i need to be sure that the transition continues and that i will are available in to support set up for clients or when there is an device improve.

In their CRADA renewal, we’re proposing to Boost greater assorted demo environments. Their diffractometer doesn’t have a large extent the place the pattern sits. They need to develop and construct some temperature version capabilities by way of a heating stage and with a bit of luck a cooling stage. i'm hoping to be concerned in this.

And these days, we've been establishing a translation mechanism so that they can analyze combinatorial samples. you can have a wafer with all sorts of variations in processing, like gradients from annealing or co-deposition, for example. I installed one linear stage last yr and that i’m putting within the second one now. they are a huge support for remote entry clients. Being capable of analyze combinatorial samples is also an important application for computing device learning, which is a existing focus of IBM in addition to Brookhaven Lab.

within the close time period, I might be an associate of NIST, which allows me to work at BMM, best my affiliation has switched to NIST. i hope to proceed at Brookhaven Lab in this way.

but in the meantime, I actually have some plans. I took a big family unit canoeing travel as much as the Boundary Waters area on the u.s.Canada border in August and should be doing more trip to talk over with family unit and pals. I also want to make stained glass and different craft-oriented artwork. I have a friend in Wading River, a physicist currently retired from Brookhaven Lab, who's a superb woodworker and has a extremely artistic, artistic creativeness. They are looking to collaborate on some tasks. I additionally like to go birding, and my younger sister and i would like to go to Texas to peer painted buntings, which is on their bucket lists.

As a U.S. department of energy office of Science consumer Facility, NSLS-II allows a collaborative, holistic strategy to boost scientific endeavors through providing free access to tremendously superior devices and exciting skills. To be trained greater about analysis capabilities and collaborations with NSLS-II group of workers, please visit the NSLS-II site.

Brookhaven national Laboratory is supported by way of the U.S. department of energy’s office of Science. The office of Science is the one biggest supporter of simple research within the physical sciences in the united states and is working to handle one of the vital most urgent challenges of their time. For greater information, visit https://power.gov/science.

comply with @BrookhavenLab on Twitter or find us on facebook.

2021-19268  |  INT/EXT  |  Newsroom

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